Imperial College London
Professor Don Craig

ProfessorDonCraig

Faculty of Natural Sciences, Department of Chemistry

Professor of Organic Synthesis
 
 
 
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Contact

 

+44 (0)20 7594 5771d.craig Website

 
 
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Location

 

501DMolecular Sciences Research HubWhite City Campus

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Summary

 

Publications

Publication Type
Year
to

110 results found

Craig D, Spreadbury SRJ, White AJP, 2020, Synthesis and hetero-diels–alder reactions of enantiomerically pure dihydro-1H-azepines, Chemical Communications, Vol: 56, Pages: 9803-9806, ISSN: 1359-7345

Thermolysis of enantiomerically pure 3-substituted 7,7-dihalo-2-azabicyclo[4.1.0]heptanes in the presence of K2CO3 gives in good yields 2-alkyl-6-halo-1-tosyl-2,3-dihydro-1H-azepines. These undergo highly stereoselective [4+2] cycloaddition reactions with heterodienophiles and arylation/alkenylation under Suzuki conditions.

Journal article

Craig D, Goldberg FW, Pett RW, Tholen NTH, White AJPet al., 2013, Aziridine-based Concise Synthesis of (±)-Alstonerine, Chemical Communications, Vol: 49, Pages: 9275-9277, ISSN: 1359-7345

A concise synthesis of the macroline-related alkaloid (±)-alstonerine 1 is reported. Key steps are regioselective and stereospecific aziridine ring-opening using a sulfone-stabilised carbanion, Me3Al-meditaed O → N-transacylation–elimination, intramolecular Michael reaction, and one-pot reduction–dehydration–Pictet–Spengler cyclisation.

Journal article

Craig D, 2013, Creating Complexity, BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY, Vol: 9, Pages: 1881-1882, ISSN: 1860-5397

Journal article

Partridge S, Craig D, Lucas A, 2011, Toward the total synthesis of 1a,25-dihydroxylumisterol, 242nd National Meeting of the American-Chemical-Society (ACS), Publisher: AMER CHEMICAL SOC, ISSN: 0065-7727

Conference paper

Camp JE, Craig D, Funai K, White AJPet al., 2011, Decarboxylative Claisen rearrangement reactions: synthesis and reactivity of alkylidene-substituted indolines, ORGANIC & BIOMOLECULAR CHEMISTRY, Vol: 9, Pages: 7904-7912, ISSN: 1477-0520

Journal article

Craig D, Funai K, Gore SJ, Kang A, Mayweg AVWet al., 2011, Transannular Claisen rearrangement reactions for the synthesis of vinylcyclobutanes: formal synthesis of (±)-grandisol, ORGANIC & BIOMOLECULAR CHEMISTRY, Vol: 9, Pages: 8000-8002, ISSN: 1477-0520

Journal article

Craig D, Harvey JW, O'Brien AG, White AJPet al., 2011, Claisen rearrangements of equilibrating allylic azides, ORGANIC & BIOMOLECULAR CHEMISTRY, Vol: 9, Pages: 7057-7061, ISSN: 1477-0520

Journal article

Chahal JK, Craig D, Smethurst CA, White AJPet al., 2011, Facile Diels-Alder dimerisation of a vinyloxepin synthesised using intramolecular ene-yne metathesis, ARKIVOC, Pages: 127-139, ISSN: 1551-7004

Journal article

Craig D, Harvey JW, O'Brien AG, White AJPet al., 2010, Exopericyclic stereocontrol in Johnson-Claisen rearrangements of allylic sulfides, CHEMICAL COMMUNICATIONS, Vol: 46, Pages: 6932-6934, ISSN: 1359-7345

Journal article

Craig D, Lu P, Mathie T, Tholen NTHet al., 2010, Directed addition of sulfur-stabilised carbanions to 1,2,3-trisubstituted aziridines, Tetrahedron, Vol: 66, Pages: 6376-6382, ISSN: 0040-4020

Thioether and sulfone-stabilised carbanions possessing varying functional groups enter into highly regioselective, stereospecific ring-opening reactions with vinyl- and hydroxymethyl-substituted aziridines. Some derivatisation reactions of the adducts are reported.

Journal article

Craig D, Lu P, White AJP, 2010, Highly diastereoselective allylation reactions of dilithiated 4-(phenylsulfonyl)-cyclopent-2-enol, TETRAHEDRON LETTERS, Vol: 51, Pages: 99-101, ISSN: 0040-4039

Journal article

Craig D, Gore SJ, Lansdell MI, Lewis SE, Mayweg AVW, White AJPet al., 2010, Transannular, decarboxylative Claisen rearrangement reactions for the synthesis of sulfur-substituted vinylcyclopropanes, CHEMICAL COMMUNICATIONS, Vol: 46, Pages: 4991-4993, ISSN: 1359-7345

Journal article

Camp JE, Craig D, 2009, Reactivity of dearomatised furans synthesised via the decarboxylative Claisen rearrangement, TETRAHEDRON LETTERS, Vol: 50, Pages: 3503-3508, ISSN: 0040-4039

Journal article

Carballares S, Craig D, Hyland CJT, Lu P, Mathie T, White AJPet al., 2009, Highly regioselective ring-opening of trisubstituted aziridines by sulfur-stabilised carbanions, CHEMICAL COMMUNICATIONS, Pages: 451-453, ISSN: 1359-7345

Journal article

Ley SV, Abad-Somovilla A, Anderson JC, Ayats C, Baenteli R, Beckmann E, Boyer A, Brasca MG, Brice A, Broughton HB, Burke BJ, Cleator E, Craig D, Denholm AA, Denton RM, Durand-Reville T, Gobbi LB, Goebel M, Gray BL, Grossmann RB, Gutteridge CE, Hahn N, Harding SL, Jennens DC, Jennens L, Lovell PJ, Lovell HJ, de la Puente ML, Kolb HC, Koot W-J, Maslen SL, McCusker CF, Mattes A, Pape AR, Pinto A, Santafianos D, Scott JS, Smith SC, Somers AQ, Spilling CD, Stelzer F, Toogood PL, Turner RM, Veitch GE, Wood A, Zumbrunn Cet al., 2008, The Synthesis of Azadirachtin: A Potent Insect Antifeedant, CHEMISTRY-A EUROPEAN JOURNAL, Vol: 14, Pages: 10683-10704, ISSN: 0947-6539

Journal article

Craig D, Paina F, Smith SC, 2008, Double decarboxylative Claisen rearrangement reactions:: microwave-assisted <i>de novo</i> synthesis of pyridines, CHEMICAL COMMUNICATIONS, Pages: 3408-3410, ISSN: 1359-7345

Journal article

Craig D, Slavov NK, 2008, A quantitative structure-reactivity relationship in decarboxylative Claisen rearrangement reactions of allylic tosylmalonate esters, CHEMICAL COMMUNICATIONS, Pages: 6054-6056, ISSN: 1359-7345

Journal article

Berry MB, Craig D, Jones PS, Rowlands GJet al., 2007, The enantiospecific synthesis of (+)-monomorine I using a 5-<i>endo</i>-trig cyclisation strategy, BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY, Vol: 3, ISSN: 1860-5397

Journal article

Craig D, Lansdell MI, Lewis SE, 2007, Highly regioselective decarboxylative Claisen rearrangement reactions of diallyl 2-sulfonylmalonates, TETRAHEDRON LETTERS, Vol: 48, Pages: 7861-7864, ISSN: 0040-4039

Journal article

Caldwell JJ, Craig D, 2007, Sulfone-mediated total synthesis of (±)-lepadiformine, ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, Vol: 46, Pages: 2631-2634, ISSN: 1433-7851

Journal article

Caldwell JJ, Craig D, East SP, 2007, Application of a 5-<i>endo</i>-trig cyclisation in the total synthesis of (+)-preussin, ARKIVOC, Pages: 67-90, ISSN: 1551-7004

Journal article

Craig D, King NP, Mountford DM, 2007, Silyl-modified Bellus-Claisen rearrangement, CHEMICAL COMMUNICATIONS, Pages: 1077-1079, ISSN: 1359-7345

Journal article

Craig D, Hyland CJT, Ward SE, 2006, Stereoselective synthesis of (-)-trachelanthamidine via palladium-catalysed intramolecular allylation, SYNLETT, Pages: 2142-2144, ISSN: 0936-5214

Journal article

Craig D, Henry GD, 2006, Total synthesis of the cytotoxic guaipyridine sesquiterpene alkaloid (+)-cananodine, EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, Vol: 2006, Pages: 3558-3561, ISSN: 1434-193X

Journal article

Bourgeois D, Craig D, Grellepois F, Mountford DM, Stewart AJWet al., 2006, A [3,3]-sigmatropic process catalysed by acetate. The decarboxylative Claisen rearrangement, TETRAHEDRON, Vol: 62, Pages: 483-495, ISSN: 0040-4020

Journal article

Craig D, King NP, Kley JT, Mountford DMet al., 2005, Heteroaromatic decarboxylative claisen rearrangement reactions, SYNTHESIS-STUTTGART, Pages: 3279-3282, ISSN: 0039-7881

Journal article

Craig D, Grellepois F, White AJP, 2005, Asymmetric decarboxylative Claisen rearrangement reactions of sulfoximine-substituted allylic tosylacetic esters, JOURNAL OF ORGANIC CHEMISTRY, Vol: 70, Pages: 6827-6832, ISSN: 0022-3263

Journal article

Cox P, Craig D, Ioannidis S, Rahn VSet al., 2005, 4-(phenylsulfonyl)-4-lithiocyclopentene as a nucleophilic 2-pentene-1,5-dial synthetic equivalent. An aziridine-based synthetic approach to (-)-alstonerine, TETRAHEDRON LETTERS, Vol: 46, Pages: 4687-4690, ISSN: 0040-4039

Journal article

Bonfanti JF, Craig D, 2005, Synthesis of substituted dihydrobenzothiopyrans and dihydrobenzopyrans by cation-mediated cyclisation reactions, TETRAHEDRON LETTERS, Vol: 46, Pages: 3719-3723, ISSN: 0040-4039

Journal article

Craig D, Henry GD, 2005, Sulfone-mediated synthesis of polysubstituted pyridines, TETRAHEDRON LETTERS, Vol: 46, Pages: 2559-2562, ISSN: 0040-4039

Journal article

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