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• Journal article
  Palomares E, Vilar R, Green A, Durrant JRet al., 2004,

  Alizarin complexone on nanocrystalline TiO2: A heterogeneous approach to anion sensing

  , ADVANCED FUNCTIONAL MATERIALS, Vol: 14, Pages: 111-115, ISSN: 1616-301X
  • Author Web Link
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  • Citations: 96
• Journal article
  Vilar R, 2004,

  Hydrogen-bonding templated assemblies

  , SUPRAMOLECULAR ASSEMBLY VIA HYDROGEN BONDS II, Vol: 111, Pages: 85-137, ISSN: 0081-5993
  • Author Web Link
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  • Citations: 22
• Journal article
  Krishnadasan S, Tovilla J, Vilar R, deMello AJ, deMello JCet al., 2004,

  On-line analysis of CdSe nanoparticle formation in a continuous flow chip-based microreactor

  , JOURNAL OF MATERIALS CHEMISTRY, Vol: 14, Pages: 2655-2660, ISSN: 0959-9428
  • Author Web Link
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  • Citations: 117
• Journal article
  Owen GR, Vilar R, White AJP, Williams DJet al., 2003,

  Studies on the reactivity of isocyanates and isothiocyanates with palladium-imidoyl complexes

  , ORGANOMETALLICS, Vol: 22, Pages: 4511-4521, ISSN: 0276-7333
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  • Citations: 28
• Conference paper
  Doxiadi E, Vilar R, White AJP, Williams DJet al., 2003,

  Anion-templated synthesis and structural characterisation of Ni/Pd-containing metalla-macrocycles

  , 223rd ACS National Meeting, Publisher: PERGAMON-ELSEVIER SCIENCE LTD, Pages: 2991-2998, ISSN: 0277-5387
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  • Citations: 38
• Journal article
  Owen GR, Vilar R, White AJP, Williams DJet al., 2003,

  Synthesis and structural characterization of a novel dipalladium complex with an unprecedented PdCN bonding motif

  , ORGANOMETALLICS, Vol: 22, Pages: 3025-3027, ISSN: 0276-7333
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  • Citations: 18
• Journal article
  Williamson AM, Owen GR, Mingos DMP, Vilar R, White AJP, Williams DJet al., 2003,

  Synthesis and structural characterisation of the palladium cluster compounds [Pd-3(mu-SO2)(2)(mu-PPh(2)py)(2)(PBz(3))(2)] and [Pd-4(mu-SO2)(2)(mu(3)-S)(CNR)(PBz(3))(4)] (R = Bu-t, 2,6-dimethylphenyl and cyclohexyl)

  , DALTON TRANSACTIONS, Pages: 2526-2532, ISSN: 1477-9226
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  • Citations: 6
• Journal article
  Vilar R, 2003,

  Anion-templated synthesis

  , ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, Vol: 42, Pages: 1460-1477, ISSN: 1433-7851
  • Author Web Link
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  • Citations: 319
• Conference paper
  Edel JB, Krishmadasan S, Tovilla cao-Romero J, Vilar R, de Mello JC, de Mello AJet al., 2003,

  Continuous real-time monitoring of quantum dot synthesis within microfluidic reactors

  , International conference on minaturized chemical and biochemical analysis systems; Micro total analysis systems 2003, Pages: 673-674
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• Conference paper
  Edel JB, Krishnadasan S, cao-Romero JT, Vilar-Compte R, de Mello JC, de Mello AJet al., 2003,

  Controlled synthesis of compound semiconductor nanoparticles using microfluidic reactors

  , New York, 12th international conference on solid-state sensors, actuators and microsystems, Boston, Massachusetts, 9 - 12 June 2003, Publisher: I E E E, Pages: 1730-1733
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• Journal article
  Owen GR, Vilar R, White AJP, Williams DJet al., 2002,

  Influence of chelating phosiphines on the insertion of isocyanides into palladium-methyl bonds in (P-P)Pd(Me)Cl complexes and their further reaction with olefins and isothiocyanates

  , ORGANOMETALLICS, Vol: 21, Pages: 4799-4807, ISSN: 0276-7333
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  • Citations: 37
• Conference paper
  Rais D, Mingos DMP, Vilar R, White AJP, Williams DJet al., 2002,

  Directing role of anions in the syntheses of the silver-alkynyl cages [Ag-14(C=(CBu)-Bu-t)(12)X][BF4] (X = FCl, Br) and silver-alkynyl polymers [Ag-3(C=(CBu)-Bu-t)(2)(X)]n (X = Tos, NO3)

  , 222nd National Meeting of the American-Chemical-Society, Publisher: ELSEVIER SCIENCE SA, Pages: 87-93, ISSN: 0022-328X
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  • Citations: 66
• Journal article
  Vilar R, Doxiadi E, Burkill HA, 2002,

  Anion templated synthesis of metalla-macrocycles.

  , ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, Vol: 223, Pages: A12-A12, ISSN: 0065-7727
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• Conference paper
  Mingos DMP, Vilar R, Rais D, 2002,

  Recent studies on alkynyl complexes of the Group 11 and 12 metals

  , International Symposium on Interactions of pi-Systems with Metals, Publisher: ELSEVIER SCIENCE SA, Pages: 126-133, ISSN: 0022-328X
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  • Citations: 55
• Journal article
  Burkill HA, Vilar R, White AJP, Williams DJet al., 2002,

  Synthesis and structural characterisation of the novel iron helicate [Fe-2(mu-L)(4)(mu-Cl)(2)][FeCl4](2) and metalla-macrocycle [Fe-2(mu-L)(2)(THF)(4)Cl-2][FeCl4](2) {L = N,N '-di(n-butylcarbamoyl)-pyridine-2,6-dicarboxamide}

  , JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, Pages: 837-839, ISSN: 1472-7773
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  • Citations: 14
• Journal article
  Rais D, Yau J, Mingos DMP, Vilar R, White AJP, Williams DJet al., 2001,

  Anion-Templated Syntheses of Rhombohedral Silver-Alkynyl Cage Compounds.

  , Angew Chem Int Ed Engl, Vol: 40, Pages: 3464-3467
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• Journal article
  Rais D, Yau J, Mingos DMP, Vilar R, White AJP, Williams DJet al., 2001,

  Anion-templated syntheses of rhombohedral silver - Alkynyl cage compounds

  , ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, Vol: 40, Pages: 3464-+, ISSN: 1433-7851
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  • Citations: 196
• Journal article
  Schweiger M, Seidel SR, Arif AM, Stang PJet al., 2001,

  The self-assembly of an unexpected, unique supramolecular triangle composed of rigid subunits

  , ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, Vol: 40, Pages: 3467-+, ISSN: 1433-7851
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  • Citations: 95
• Journal article
  Cheng ST, Doxiadi E, Vilar R, White AJP, Williams DJet al., 2001,

  Anion templated synthesis of Ni/Pd containing metalla-macrocycles

  , JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, Pages: 2239-2244, ISSN: 1472-7773
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  • Citations: 49
• Journal article
  Dura-Vila V, Mingos DMP, Vilar R, White AJP, Williams DJet al., 2000,

  Insertion of O2 into a Pd(I)-Pd(I) dimer and subsequent C-O bond formation by Activation of a C-H bond

  , Chemical Communications, Pages: 1525-1526, ISSN: 1359-7345
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• Journal article
  Rais D, Mingos DMP, Vilar R, White AJP, Williams DJet al., 2000,

  -coordination of silver and copper to mercury bis-alkynyls: synthesis and structural characterisation

  , Organometallics, Vol: 19, Pages: 5209-5217, ISSN: 0276-7333
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• Journal article
  Dura-Vila V, Mingos DMP, Vilar R, White AJP, Williams DJet al., 2000,

  Reactivity studies of[Pd2(-X)2(PBut3)2 (X=Br,I) with CNR (R=2,6-dimethylphenyl), H2 and alkynes

  , Journal of Organometallic Chemistry, Vol: 600, Pages: 198-205, ISSN: 0022-328X
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• Journal article
  Arifhodzic-Radojevic S, Burrows AD, Choi N, McPartlin M, Mingos DMP, Tarlton SV, Vilar Ret al., 1999,

  Reactivity of the palladium dimer [Pd<inf>2</inf>(μ-SO<inf>2</inf>)(μ-dba)(PBz<inf>3</inf>)<inf>2</inf>]. Syntheses and structural characterisation of [Pd<inf>3</inf>(μ-SO<inf>2</inf>)<inf>3</inf>(PBz<inf>3</inf>)<inf>3</inf>], [Pd<inf>2</inf>(μ-SO<inf>2</inf>)(μ-dppm)(PBz<inf>3</inf>)<inf>2</inf>], [Pd(SO<inf>2</inf>)(PBz<inf>3</inf>)<inf>2</inf>]

  , Journal of the Chemical Society - Dalton Transactions, Pages: 3981-3988, ISSN: 0300-9246

  The reaction between [Pd2(dba)3]·solvent (dba = dibenzylideneacetone, solvent = CHCl3 or C6H6) and PBz3 (Bz = benzyl) in the presence of SO2 led to either [Pd2(μ-SO2)(μ-dba)(PBz3)2] 1 or [Pd3(μ-SO2)3(PBz3)3] 2 depending on the absence or presence of an excess of SO2 in solution or in the recrystallisation. The crystal structure of 2 shows it to be a regular triangulo-cluster with Pd-Pd bond distances 2.7225(9) Å. Complex 1 reacted with dppm with displacement of dba to give [Pd2(μ-SO2)(μ-dppm)(PBz3)2] 3. The crystal structure of 3 shows it to have a much shorter Pd-Pd bond length than 1 [2.670(2) Åfor 3 cf. 2.885(2) Å for 1], which can be rationalised on the basis of the palladium atoms having been formally oxidised to PdI and the SO2 reduced to SO22-. Complex 1 reacted with PBz3 to give two mononuclear complexes, the previously characterised [Pd(dba)(PBz3)2] and the new complex [Pd(SO2)(PBz3)2] 4 which was characterised by a single crystal X-ray analysis. Complex 4 forms a distorted T-shaped structure with the P-Pd-P angle 163.67(14)°. It contains a η1-pyramidal SO2 ligand, and is the first mononuclear palladium SO2 complex to be crystallographically characterised. Complex 1 reacts with CO to give a mixture of the triangulo-clusters [Pd3(μ-CO)2(μ-SO2)(PBz3) 3] 5 and [Pd3(μ-CO)(μ-SO2)2(PBz3) 3] 6. Reaction with an excess of CO converted 6 into 5, and the crystal structure of 5 reveals relatively short Pd-Pd bond lengths consistent with a 42-electron cluster. Complex 1 reacted with CNBut to give [Pd3(μ-SO2)2(CNBut) 2(PBz3)3] which has also been crystallographically characterised. © The Royal Society of Chemistry 1999.

  • Abstract
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  • Citations: 19
• Journal article
  Arifhodzic-Radojevic S, Burrows AD, Choi N, McPartlin M, Mingos DMP, Tarlton SV, Vilar Ret al., 1999,

  Reactivity of the palladium dimer [Pd-2(mu-SO2)(mu-dba)(PBz(3))(2)]. Syntheses and structural characterisation of [Pd-3(mu- SO2)(3)(PBz(3))(3)], [Pd-2(mu-SO2)(mu-dppm)(PBz(3))(2)], [Pd(SO2)(PBz(3))(2)], [Pd-3(mu-CO)(2)(mu-SO2)(PBz(3))(3)] and [Pd- 3(mu-SO2)(2)(CNBut)(2)(PBz(3))(3)] (Bz = benzyl)

  , Journal of the Chemical Society-Dalton Transactions, Pages: 3981-3988, ISSN: 0300-9246
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• Journal article
  Tarlton SV, Choi N, McPartlin M, Mingos DMP, Vilar Ret al., 1999,

  Synthesis and structural characterisation of the novel tetranuclear cluster compound [Pd-4(mu-SO2)(2)(mu(3)-S)(CO)(PBz(3))(4)] (Bz=C6H5CH2)

  , Journal of the Chemical Society-Dalton Transactions, Pages: 653-654, ISSN: 0300-9246
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• Journal article
  Vilar R, Mingos DMP, White AJP, Williams DJet al., 1999,

  Aufbau synthesis of a mixed-metal anion receptor cage

  , Chemical Communications, Pages: 229-230, ISSN: 1359-7345
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• Journal article
  Burrows AD, Choi N, McPartlin M, Mingos DMP, Tarlton SV, Vilar Ret al., 1999,

  Syntheses and structural characterisation of the compounds [Pd(dba)L- 2] (where L = PBz(3) and PPh2Np) and the novel dimer [Pd-2(mu- dba)(mu-SO2)(PBz(3))(2)]

  , Journal of Organometallic Chemistry, Vol: 573, Pages: 313-322, ISSN: 0022-328X
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• Journal article
  Long NJ, Martin AJ, Vilar R, White AJP, Williams DJ, Younus Met al., 1999,

  Synthesis, characterization, and theoretical studies of new alkynylferrocene and -biferrocene ligands and their platinum- containing dimers and oligomers

  , Organometallics, Vol: 18, Pages: 4261-4269, ISSN: 0276-7333
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• Journal article
  Mingos DMP, Vilar R, 1998,

  Synthesis and reactivity of palladium cluster compounds

  , Journal of Organometallic Chemistry, Vol: 557, Pages: 131-142, ISSN: 0022-328X
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• Journal article
  Vilar R, Mingos DMP, White AJP, Williams DJet al., 1998,

  Anion control in the self-assembly of a cage coordination complex

  , Angewandte Chemie-International Edition in English, Vol: 37, Pages: 1258-1261, ISSN: 1433-7851
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